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dc.contributor.authorAltıokka, Barış
dc.contributor.authorBaykul, Mevlana Celalettin
dc.contributor.authorAltıokka, Mehmet Rıza
dc.date.accessioned2022-09-26T06:01:05Z
dc.date.available2022-09-26T06:01:05Z
dc.date.issued2013en_US
dc.identifier.citationAltıokka, B., Baykul, M. C., & Altıokka, M. R. (2013). Some physical effects of reaction rate on PbS thin films obtained by chemical bath deposition. Journal of crystal growth, 384, 50-54.en_US
dc.identifier.issn0022-0248
dc.identifier.issn1873-5002
dc.identifier.urihttps://doi.org/10.1016/j.jcrysgro.2013.09.003
dc.identifier.urihttps://hdl.handle.net/11552/2592
dc.description.abstractThin films of polycrystalline lead sulfide (PbS) have been deposited on glass substrates at 303±1 K using chemical bath deposition (CBD). The precipitation of PbS on solid surfaces under four different reaction conditions was performed using a sodium sulfite (Na2SO3) compound as an inhibitor. The kinetics model for the reaction between Pb2+ and S2− was developed according to the amounts of Pb2+ concentrations measured by atomic absorption spectroscopy (AAS) during the precipitation of PbS. The surface morphologies of PbS thin films were studied with a Scanning Electron Microscope (SEM). It was found that the precipitation rate effects the formation of pinhole. To obtain a good quality of thin films the optimum concentration of lead nitrate (Pb(NO3)2), sodium hydroxide (NaOH), thiourea (CS(NH2)2) and Na2SO3 in the final solution was determined to be 0.0089, 0.1460, 0.510 and 0.00023 M, respectively. The film structures were characterized by X-ray diffractometer (XRD). The XRD results showed that the films formed galena cubic structures which represent the natural mineral of PbS. The crystallite sizes of the films were found to be between 23 and 37 nm.en_US
dc.language.isoengen_US
dc.publisherElsevieren_US
dc.identifier.doi10.1016/j.jcrysgro.2013.09.003en_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectX-ray Diffractionen_US
dc.subjectGrowth From Solutionsen_US
dc.subjectPolycrystalline Depositionen_US
dc.subjectSemiconducting Materialsen_US
dc.titleSome physical effects of reaction rate on PbS thin films obtained by chemical bath depositionen_US
dc.typearticleen_US
dc.relation.ispartofJournal of Crystal Growthen_US
dc.departmentMeslek Yüksekokulları, Meslek Yüksekokulu, Elektrik ve Enerji Bölümüen_US
dc.authorid0000-0001-8891-973Xen_US
dc.identifier.volume384en_US
dc.identifier.startpage50en_US
dc.identifier.endpage54en_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.relation.indexScopusen_US
dc.relation.indexWoSen_US
dc.relation.indexWoS - Science Citation Index Expandeden_US
dc.contributor.institutionauthorAltıokka, Barış
dc.description.wospublicationidWOS:000326680900010en_US
dc.description.scopuspublicationid1-s2.0-S0022024813005897en_US
dc.description.wosqualityQ3en_US
dc.description.wosqualityQ2en_US


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